A novel laboratory set-up for investigating surface and interface reactions during short term annealing cycles at high temperatures

Auinger, M.; Vogel, D.; Vogel, A.; Spiegel, M.; Rohwerder, M.
August 2013
Review of Scientific Instruments;Aug2013, Vol. 84 Issue 8, p085108
Academic Journal
High temperature oxidation is an important research discipline that covers many topics in steel manufacture and modern energy research. To account for the need of adjusting accurate processing conditions, recent developments of the high temperature laboratory setup at the Max-Planck-Institut für Eisenforschung GmbH will be presented. The experimental assembly has been optimized to investigate surface and interface reactions at elevated temperatures in low oxygen activity gases, covering a large field of experimental possibilities. Many efforts have been taken to enable an accurate control and in situ monitoring of process conditions such as gas flow, gas composition, impurity content, and mass change of the sample.


Related Articles

  • Chemical oxidation of lithium-containing aluminum alloy 1424. Oleinik, S.; Zimina, Yu.; Karimova, S.; Tararaeva, T. // Protection of Metals & Physical Chemistry of Surfaces;Dec2010, Vol. 46 Issue 7, p812 

    The possibility of obtaining protective conversion coatings on the surface of lithium-containing aluminum alloy 1424 in chromate-free conversion solutions IFKhANAL-1 and IFKhANAL-3 is shown. The kinetics of formation, composition, and protective properties of these coatings are studied. It is...

  • Evaluation of Cyclic Oxidation and Hot Corrosion Behavior of HVOF-Sprayed WC-Co/NiCrAlY Coating. Somasundaram, B.; Kadoli, Ravikiran; Ramesh, M. // Journal of Thermal Spray Technology;Aug2014, Vol. 23 Issue 6, p1000 

    Corrosion of metallic structural materials at an elevated temperature in complex multicomponent gas environments are potential problems in many fossil energy systems, especially those using coal as a feedstock. Combating these problems involves a number of approaches, one of which is the use of...

  • Chemical Oxidation of an АМг-3 Type Alloy in Alkaline Molybdate-Containing Solutions. Kuznetsov, Yu. I.; Oleinik, S. V.; Khaustov, A. V. // Protection of Metals;Jul/Aug2003, Vol. 39 Issue 4, p311 

    A possibility to obtain conversion coatings (CCs) on an АМг-3 type aluminum alloy from alkaline molybdate-containing solutions (pH 12.8) is studied instead of its chromating. The effect of converting solution components on the resistance of thus obtained CCs to local anodic activation...

  • Welding Niobium Alloys. Mertz, James // Welding Journal;Nov2003, Vol. 82 Issue 11, p38 

    Focuses on the characteristics, capabilities and practices for fabrication of niobium alloys. Benefits of using niobium alloys; Sensitivity of niobium alloys to oxidation at high temperature; Susciptibility of niobium to intergranular corrosion at elevated temperature.

  • Deterioration of tin-rich organ pipes. Chiavari, C.; Martini, C.; Poli, G.; Prandstraller, D. // Journal of Materials Science;Mar2006, Vol. 41 Issue 6, p1819 

    Tin-rich organ pipes are often affected by localised deterioration in the form of grey pustules, pinholes, cracks and exfoliations at the surface. Two main types of decay of tin-base materials that might have a similar appearance, i.e. the surface of the object covered with dark grey pustules,...

  • Development of nickel incorporated aluminum alloy matrix as an efficient sacrificial anode. Shibli, S.; Dilimon, V.; Mohan, Asha // Journal of Applied Electrochemistry;Sep2007, Vol. 37 Issue 9, p1015 

    Al–Zn + Ni matrix anodes were fabricated using Ni as activator. The Al–Zn + Ni anodes had good physico-chemical characteristics. Reinforcement by Ni resulted in improvement in grain size of the metal–metal matrix. The effect of Ni on the galvanic performance of the anodes...

  • Corrosion behavior of 2099 Al–Li alloy in NaCl aqueous solution. Chen, Bin; Li, Chao-Hao; He, Shi-Chen; Li, Xiao-ling; Lu, Chen // Journal of Materials Research;Jun2014, Vol. 29 Issue 12, p1344 

    The corrosion behavior of 2099 Al–Li alloy in NaCl aqueous solutions with different concentrations (1.5, 3.5, and 5.0% in mass fraction) was investigated. Its corrosion resistance was evaluated using electrochemical measurements together with full immersion tests. The results showed that...

  • Fabrication of metallic nanowire arrays by electrodeposition into nanoporous alumina membranes: effect of barrier layer. Sharma, Gaurav; Pishko, Michael V.; Grimes, Craig A. // Journal of Materials Science;Jul2007, Vol. 42 Issue 13, p4738 

    Deposition into nanoporous alumina membranes is widely used for nanowire fabrication. Herein using AC electrodeposition ternary Fe–Co–Ni nanowires are fabricated within the nanoscale-pores of alumina membranes. Using an electrodeposition frequency of 1,000 Hz, 15 Vrms, consistently...

  • Transport of gaseous and dense carbon dioxide in pipelines: is there an internal corrosion risk? Sandana, Daniel; Hadden, Matthew; Race, Julia; Charles, E. A. // Journal of Pipeline Engineering;Sep2012, Vol. 11 Issue 3, p229 

    Transporting anthropogenic CO2 in pipelines is an essential component in the realization and implementation of carbon capture and storage (CCS). Transportation of dense CO2 has generally been the preferred economic solution, but projects in the UK have also considered transportation of gaseous...


Read the Article


Sorry, but this item is not currently available from your library.

Try another library?
Sign out of this library

Other Topics